Xylene 106 -47.8 140 0. Experimental. To start the experiment, 0.289 g of anthracene and 0.16 g of maleic anhydride were put into a 5 mL round bottom flask. Then, 3 mL of xylene was added to the mixture and stirred.
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Since the reaction involves four π electrons in the diene and Anthracene acts as the diene and maleic anhydride functions as the dienophile. Xylene (dimethylbenzene) is used as a high boiling temperature solvent so that the reaction will proceed quickly. Melting temperature analysis will be used to characterize the product. The Diels-Alder Reaction of Anthracene with Maleic Anhydride - Lu Le Laboratory The Diels-Alder reaction is a cycloaddition reaction, a reaction in which two molecules undergo addition to yield a cyclic product. – Diels Alder Reaction Of Anthracene With Maleic Anhydride Lab Report The very first thing that you need to do is to decide what type of information you require to include in your excellent laboratory report sample. Molecular and crystal structure of the adduct of anthracene with maleic anhydride. Journal of Structural Chemistry 1980, 20 (5) , 755-759.
Anthracene-maleic anhydride diels-alder adduct (5443-16-3), Wholesale Various High Quality Anthracene-maleic anhydride diels-alder adduct (5443-16-3) Products from Global Sodium Tripolyphosphate Suppliers and Anthracene-maleic anhydride diels-alder adduct (5443-16-3) Factory,Importer,Exporter at Okchem.com. 3) maleic anhydride (dienophile) anthracene adduct) (diene) The reaction is carried out in xylene, which is actually a mixture of the three dimethylbenzenes, for three reasons.
Spectral Code of Anthracene with. Maleic Anhydride prepared by L. G. Wade, Jr., Whitman College. Use the Diels-Alder reaction to form a bridged polycyclic anhydride.
Actually used 2.79 grams of 3-sulfolene and 1.63 grams maleic anhydride. 2.79 grams C 4 H 6 O 2 S x = 0.0236 mol C 4 H 6 O 2 S = 0.0236 mol C 4 H 6
Similar Compounds. Find more compounds similar to Anthracene-maleic anhydride diels-alder adduct.. Note: Cheméo is only indexing the data, follow the source links to retrieve the latest data. The source is also providing more information like the publication year, authors and more. Anthracene-maleic anhydride diels-alder adduct contains total 33 atom(s); 12 Hydrogen atom(s), 18 Carbon atom(s) and 3 Oxygen atom(s).
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Essay text: Anthracene was the diene and maleic anhydride was the dienophile.
Essay text: Anthracene was the diene and maleic anhydride was the dienophile. The percent yield of the crude product was 69.03%. Following recrystallization of the product using xylene and vacuum filtration, a percent yield of 37.42% for the recrystallized product was collected. Hand-drawn Arrow Pushing Mechanism of anthracene and maleic anhydride to 9,10-dihydroanthracene-9,10-GB-succinic acid anhydride (4 pts.): NMR Assignments (4 pts, total) Draw the structure of 9.10-dihydroanthracene-9,10-B-succinic acid anhydride (label the protons with lowercase letters from the NMR spectrum found in the Online Experiment Video section) (4 pts.)
Theoretical Yield of 4-cyclohexene-cis-1,2-dicarboxylic anhydride = moles of limiting reactant (maleic anhydride) x molar weight of 4-cyclohexene-cis-1,2-dicarboxylic anhydride.
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While the product is not an insecticide and does not Figure 2. Reaction to form cis -Norbornene-5,6-endo -dicarboxylic anhydride (Pavia 417).
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Anthracene with Maleic Anhydride The Diels-Alder reaction is a member of a class of reactions called cycloadditions. The reaction involves three π bonds, two from the diene and one from the dienophile in a concerted reaction to form a six-membered ring. Since the reaction involves four π electrons in the diene and Anthracene acts as the diene and maleic anhydride functions as the dienophile. Xylene (dimethylbenzene) is used as a high boiling temperature solvent so that the reaction will proceed quickly. Melting temperature analysis will be used to characterize the product.